Optimization of the Mixing of Hibiscus Flower (Hibiscus rose sinensis) Extract as a Lip Balm Color with Variations in Concentration

Diah Indah Kumala Sari, Fransisca Dita Mayangsari, Fransisca Dita Mayangsari, Elasari Dwi Pratiwi

Abstract


Hibiscus rosa sinensis L. is widely used by the community to decorate the garden because of its splendor. In addition, Hibiscus flowers containing anthocyanin and flavonoids have antioxidants, which function as antioxidants against free radicals. This natural dye can be obtained by extracting Hibiscus flowers through maceration using 96% ethanol. In this research, Hibiscus flowers were obtained from Sendang Rejo Village, Lamongan Regency. In the extract process, the Hibiscus flower’s petals were blended until smooth, then added to 96% ethanol (1 liter) and stirred for 30 minutes. Filtrate results were taken, placed in a porcelain dish, and put in an oven at 60 °C for a day. Four formulas were made with varying levels of Hibiscus flower extract: F1 (0%), F2 (2%), F3 (4%), and F4 (6%). Physical evaluation included organoleptic, homogeneity, dispersibility, pH, and qualitative tests for the identification of anthocyanins. The results of the organoleptic, homogeneity, dispersion, pH, and identification of anthocyanins evaluations were then analyzed descriptively. The data from the organoleptic test indicated that F1 had an odorless white color, while F2, F3, and F4 had a red and white color with a distinctive Hibiscus flower aroma. The homogeneity test revealed that while F1 had good homogeneity, F2, F3, and F4 were not homogeneous (heterogeneous). The spreadability test on the four formulas did not fall within the range of requirements, namely 5-7 cm, with an average value of 3.53, but this was related to several significant reasons. In addition, the pH test results matched the requirements for topical preparations, namely 4.5–6.5, with an average value of 5.075. In conclusion, Hibiscus flower extract obtained through the maceration method with 96% ethanol could not give a homogeneous red color from the anthocyanin substance. Physical evaluation and anthocyanin identification tests also obtained good results.

Keywords


Anthocyanin; Hibiscus flowers; lip balm; physical evaluation

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References


Mawazi SM, Azreen Redzal NAB, Othman N, Alolayan SO. Lipsticks history, formulations, and production: A narrative review. Cosmetics. 2022;9(1):25. http://dx.doi.org/10.3390/cosmetics9010025

Kadu M, Vishwasrao S, Singh S. Review on Natural Lip Balm. International Journal of Research in Cosmetic Science. International Journal of Research in Cosmetic Science. 2014;5(1):1–7.

II E.Kodeks Kosmetika Indonesia. Indonesia; 2012.

Sarfaraz KN. Pharmaceutical Manufacturing Formulations Semisolid Products. New York, Washington DC; 2004.

Ngan LTM, Tan MT, Hoang NVM, Thanh DT, Linh NTT, Hoa TTH, et al. Antibacterial activity of Hibiscus rosa-sinensis L. red flower against antibiotic-resistant strains of Helicobacter pylori and identification of the flower constituents. Braz J Med Biol Res. 2021;54(7). http://dx.doi.org/10.1590/1414-431x2020e10889

Zhelsiana DA, Pangestuti YS, Nabilla F, Lestari NP, Wikantyasning ER. Formulasi dan Evaluasi Sifat Fisik Masker Gel Peel-Off Lempung Bentonite. The 4th University Research Colloquium [Internet]. 2016;42–5. Available from: http://hdl.handle.net/11617/7730

Kase MG, Prasetyaningsih A, Aditiyarini D. Antioxidant and antibacterial activity of pomegranate extract (Punica granatum L.) in lip balm formulation. Biol Med Nat Prod Chem. 2023;12(1):109–17. http://dx.doi.org/10.14421/biomedich.2023.121.109-117

Sáyago-Ayerdi SG, Arranz S, Serrano J, Goñi I. Dietary fiber content and associated antioxidant compounds in Roselle flower (hibiscus sabdariffaL.) beverage. J Agric Food Chem. 2007;55(19):7886–90 http://dx.doi.org/10.1021/jf070485b

Ali BH, Wabel NA, Blunden G. Phytochemical, pharmacological and toxicological aspects ofHibiscus sabdariffa L.: a review. Phytother Res. 2005;19(5):369–75. http://dx.doi.org/10.1002/ptr.1628

He XL, Li XL, Lv YP, He Q. Composition and color stability of anthocyanin-based extract from purple sweet potato. Food Sci Technol. 2015;35(3):468–73. http://dx.doi.org/10.1590/1678-457x.6687

Riniati R, Sularasa A, Febrianto AD. Ekstraksi Kembang sepatu (Hibiscus Rosa Sinensis L) Menggunakan Pelarut Metanol dengan Metode Sokletasi untuk Indikator Titrasi Asam Basa. Ind J Chem Anal. 2019;2(01). http://dx.doi.org/10.20885/ijca.vol2.iss1.art5

Vilas Boas AC, Henrique P de C, Lima LC de O, Decarlos Neto A. Antioxidant activity, anthocyanins and organic acids content of grape juices produced in Southwest of Minas Gerais, Brazil. Ciênc Agrotecnologia. 2014;38(5):480–6. http://dx.doi.org/10.1590/s1413-70542014000500007

Inggrid HM, Jaka, Santoso H. Natural red dyes extraction on roselle petals. IOP Conf Ser Mater Sci Eng. 2016;162(1):012029. http://dx.doi.org/10.1088/1757-899x/162/1/012029

Amperawati S, Hastuti P, Pranoto Y, Santoso U. Efektifitas Frekuensi Ekstraksi Serta Pengaruh Suhu dan Cahaya Terhadap Antosianin dan Daya Antioksidan Ekstrak Kelopak Rosella (Hibiscus sabdariffa L.). J Apl Teknol Pangan. 2019;8(1). http://dx.doi.org/10.17728/jatp.3527

Chakraborty S, Majumder S, Ghosh A, Bhattacharya M. Comprehensive profiling of aroma imparting biomolecules in foliar extract of Hibiscus fragrans Roxburgh: a metabologenesis perspective. J Biomol Struct Dyn. 2022;40(20):10345–58. http://dx.doi.org/10.1080/07391102.2021.1943525

Sampebarra AL. Mempelajari Kestabilan dan Efek Iritasi Sediaan Lipstik yang Diformulasi dengan Lemak Kakao. Jurnal Industri Hasil Perkebunan. 2016;11(2):97. http://dx.doi.org/10.33104/jihp.v11i2.3420

Dyah P, Ratih, Pangestu M. Archives Pharmacia Volume 2 Nomor 2. Formulasi dan Evaluasi sediaan Balsam Bibir Menggunakan ekstrak Bunga Kembang Sepatu (Hibiscus rose sinensis L) sebagai Pewarna Alami. 2020;2.

Mahalingam R, Li X, Jasti BR. Semisolid dosages: Ointments, creams, and gels. Pharmaceutical Manufacturing Handbook. Wiley; 2008. p. 267–312. http://dx.doi.org/10.1002/9780470259818.ch9

Kadu M, Suruchi V, Sonia S. Review on Natural Lip Balm. International Journal of Research in Cosmetic Science. 2014;5(1).

TRI, Dela Amalia; Chaidir, Chaidir; Hanafi, Muhammad. Moisturizing Effectiveness Of Organic Lip Cream Formulation With Beetroot Extract (Beta Vulgaris L) And Chia Seed Oil (Salvia hispanica). Media Bina Ilmiah, 2022, 17.5: 837-846

Nastiti GP, Qosim A, Puspitaningrum N, Fuadi MNN. Formula Optimization From Halal Lip Cream Variety With Tomato Extract (Lycopersicum esculentum L.). J Islam Pharm. 2023;8(1):14–7. http://dx.doi.org/10.18860/jip.v8i1.18944

Spreding of Semisolid Formulations an Update.

Ambari Y, Hapsari FND, Ningsih AW, Nurrosyidah IH, Sinaga B. Studi Formulasi Sediaan Lip Balm Ekstrak Kayu Secang (Caesalpinia sappan L.) dengan Variasi Beeswax. J Islam Pharm. 2020;5(2):36–45. http://dx.doi.org/10.18860/jip.v5i2.10434

Yusof, atuyah athirah binti, et al. Production of lip balm from stingless bee honey. 2018.

Sunnah I, Mulasih WS, Mariani S, Erwiyani AR. Uji Stabilitas Formula Optimal Sediaan Topikal Ekstrak Biji Labu Kuning (Cucurbita Maxima). Avicenna : Journal of Health Research . 2019;2(1). http://dx.doi.org/10.36419/avicenna.v2i1.259




DOI: https://doi.org/10.18196/jfaps.v4i1.16179

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